Könyv Biogenic Amines Mardiana Saaid

Biogenic Amines

Sample Preparation Techniques for Food Analysis

Nyelv: Angol
Kötés: Puha kötésű
Elérhetőség: Kiadói készleten rendelésre
Küldés 17-27 napon belül
20 540 Ft
Biogenic amines (BA) have been extensively studied in recent years due to their potential toxicity a...

Információk a könyvről

Nyelv
Angol
Kötés
Könyv - Puha kötésű
Kiadva
2010
oldal
132
EAN
9783639285291
Enbook ID
06835681
Súly
213
Méretek
150 x 220 x 8

Teljes leírás

Biogenic amines (BA) have been extensively studied in recent years due to their potential toxicity and possible use as chemical markers for assessing food quality and in cancer research. The BA were determined in 62 foods commonly consumed in Malaysia. Three sorbent materials; A18C6-MS, DA18C6-MS and AB18C6-MS were also prepared by the chemical immobilization of the crown ether ligands onto mesoporous silica support. The sorbents have been evaluated for the extraction of five BA (TRP, PUT, HIS, TYR, SPD) by the batch sorption and column method. Results obtained showed that all the sorbents exhibit highest selectively towards SPD compared to other BA. AB18C6-MS offers the higher extraction of SPD in the presence of other BA. The applicability of the proposed method for the selective extraction of SPD was demonstrated by the reasonable recoveries attained from both methods (71.2-99.8 %). Miniaturized sample preparation technique based on hollow fiber LPME with in situ derivatization using dansyl chloride also has been successfully developed for the determination of BA in foods. Under the optimized conditions, enrichment factors from 47 to 456 was achieved.

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