Modified Biginelli-type reaction with various metallophthalocyanines

Name: Modified Biginelli-type reaction with various metallophthalocyanines
Brand: LAP Lambert Academic Publishing
SKU: 9783659956720
Price: 10002 HUF
Availability: InStock

Szerző: Naceur HAMDI

Nyelv:

Kötés: Puha kötésű

Kiadó: LAP Lambert Academic Publishing

Elérhetőség: Beszállítói készleten

Küldés 5-8 napon belül

10 002 Ft

In this study, novel phthalonitriles 3,13,14 and their corresponding metal-free 4 and metallo phthal...

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Szerző

Naceur HAMDI

Nyelv

Angol

Kötés

Könyv - Puha kötésű

Kiadva

2016

oldal

EAN

9783659956720

Enbook ID

15201383

Kiadó

LAP Lambert Academic Publishing

Súly

113

Méretek

150 x 220 x 4

Teljes leírás

In this study, novel phthalonitriles 3,13,14 and their corresponding metal-free 4 and metallo phthalocyanine derivatives (5,6,7,15,16,17,18) bearing differents groups were synthesized and characterized. 3,4-dihydropyrimidinones have been synthesized in good yields by a modified Biginelli-type reaction with various metallophthalocyanines 8-23 as catalysts. Among the various metallophthalocyanines studied, cobalt(II)- phthalocyanine was found to be most active for this transformation. The newly prepared compounds were characterized using elemental analyses,MS, IR, 1H/13C NMR, and UV-vis spectroscopy. In addition; the 3,4-dihydropyrimidinones 8-12 were investigated for anti-oxidant activities by super oxide radical; DPPH (2,2-Diphenyl-1-picrylhydrazyl); and hydroxyl radical scavenging assays; in which most of them displayed significant antioxidant activities. Furthermore; compounds 8-12 were evaluated for anti-inflammatory activity by indirect haemolytic and lipoxygenase inhibition assays and revealed good activity.

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Modified Biginelli-type reaction with various metallophthalocyanines

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